Effective Route to Graphitic Carbon Nitride from Ball-Milled
Amorphous Carbon in NH<suB>3</suB> Atmosphere Under Annealing

Chin. Phys. Lett.

2003, Vol. 20

Issue (9): 1554-1557 DOI:

Original Articles

Effective Route to Graphitic Carbon Nitride from Ball-Milled Amorphous Carbon in NH₃ Atmosphere Under Annealing

FEI Zhen-Yi;LIU Yu-Xian

College of Materials Science and Engineering, Shandong University, Ji’nan 250061

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FEI Zhen-Yi, LIU Yu-Xian 2003 Chin. Phys. Lett. 20 1554-1557

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Abstract Graphitic carbon nitride (g-C₃N₄) powders were successfully synthesized from ball-milled amorphous carbon under NH₃ atmosphere at high temperature, for the first time to our knowledge. The combined characteristic data obtained by x-ray diffraction, high-resolution transmission electron microscopy, electron energy loss spectroscopy, Raman spectroscopy, energy dispersive spectroscopic analysis, and Fourier transformation infrared spectroscopy provide substantial evidence for the graphite-like sp²-bonded structure with C₃N₄ stoichiometry.

Keywords: 61.82.Rx 81.07.Bc 68.37.Lp

Published: 01 September 2003

PACS:	61.82.Rx	(Nanocrystalline materials)
	81.07.Bc	(Nanocrystalline materials)
	68.37.Lp	(Transmission electron microscopy (TEM))

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https://cpl.iphy.ac.cn/ OR https://cpl.iphy.ac.cn/Y2003/V20/I9/01554

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