Chin. Phys. Lett.  2009, Vol. 26 Issue (4): 046801    DOI: 10.1088/0256-307X/26/4/046801
CONDENSED MATTER: STRUCTURE, MECHANICAL AND THERMAL PROPERTIES |
Fabrication and Characterization of Si Nanocrystals Synthesized by Electron Beam Evaporation of Si and SiO2 Mixture
LI Wei-Long, JIA Rui, LIU Ming, CHEN Chen, XIE Chang-Qing, ZHU Chen-Xin, LI Hao-Feng, ZHANG Pei-Wen, YE Tian-Chun
Key Laboratory of Nanofabrication and Novel Devices Integrated Technology, Institute of Microelectronics, Chinese Academy of Sciences, Beijing 100029
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LI Wei-Long, JIA Rui, LIU Ming et al  2009 Chin. Phys. Lett. 26 046801
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Abstract Silicon nanocrystals synthesized by electron beam (e-beam) evaporation of Si and SiO2 mixture are studied. Rutherford backscattering spectrometry of the as-deposited Si-rich silicon dioxide or oxide (SRO) thin film shows that after evaporation, the Si and SiO2 concentration is well kept, indicating that the e-beam evaporation is suitable for evaporating mixtures of Si and SiO2. The SRO thin films are annealed at different temperatures for two hours to synthesize silicon nanocrystals. For the sample annealed at 1050°C, silicon nanocrystals with different sizes and the mean diameter of 4.5nm are evidently observed by high resolution transmission electron microscopy (HRTEM). Then the Raman scattering and photoluminescence spectra arising from silicon nanocrystals are further confirmed the above results
Keywords: 68.37.Lp      73.22.-f      78.66.-w      78.67.-n     
Received: 25 September 2008      Published: 25 March 2009
PACS:  68.37.Lp (Transmission electron microscopy (TEM))  
  73.22.-f (Electronic structure of nanoscale materials and related systems)  
  78.66.-w (Optical properties of specific thin films)  
  78.67.-n (Optical properties of low-dimensional, mesoscopic, and nanoscale materials and structures)  
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https://cpl.iphy.ac.cn/10.1088/0256-307X/26/4/046801       OR      https://cpl.iphy.ac.cn/Y2009/V26/I4/046801
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LI Wei-Long
JIA Rui
LIU Ming
CHEN Chen
XIE Chang-Qing
ZHU Chen-Xin
LI Hao-Feng
ZHANG Pei-Wen
YE Tian-Chun
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