摘要Pd77.5Cu6Si16.5(at.%) bulk metallic glass with a diameter up to 11 mm was successfully fabricated by water quenching method together with melt purification. By using x-ray diffraction and transmission electron microscopy techniques, the structure of the as-prepared sample is confirmed to be glassy. The resulted sample with 11 mm diameter indicates that the melt purification by fluxing method can effectively enhance the glass forming ability of Pd-Cu-Si alloy, and increase its critical size of glassy sample.
Abstract:Pd77.5Cu6Si16.5(at.%) bulk metallic glass with a diameter up to 11 mm was successfully fabricated by water quenching method together with melt purification. By using x-ray diffraction and transmission electron microscopy techniques, the structure of the as-prepared sample is confirmed to be glassy. The resulted sample with 11 mm diameter indicates that the melt purification by fluxing method can effectively enhance the glass forming ability of Pd-Cu-Si alloy, and increase its critical size of glassy sample.
DING Hong-Yu;LI Yang;YAO Ke-Fu. Preparation of a Pd-Cu-Si Bulk Metallic Glass with a Diameter up to 11mm[J]. 中国物理快报, 2010, 27(12): 126101-126101.
DING Hong-Yu, LI Yang, YAO Ke-Fu. Preparation of a Pd-Cu-Si Bulk Metallic Glass with a Diameter up to 11mm. Chin. Phys. Lett., 2010, 27(12): 126101-126101.
[1] Greer A L 1995 Science 267 1947
[2] Inoue A 2000 Acta Mater. 48 279
[3] Inoue A, Nishiyama N and Kimura H M 1997 Mater. Trans. JIM 38 179 [4] Johnson W L 1996 Mater. Sci. Forum 225–227 35
[5] Nishiyama N, Takenaka K, Wada T, Kimura H M and Inoue A 2005 Mater. Trans. JIM 46 2807
[6] Inoue A and Zhang T 1996 Mater. Trans. JIM 37 185 [7] Zheng Q, Xu J and Ma E 2007 J. Appl. Phys. 102 113519
[8] Zhang W, Zhang Q S, Qin C L and Inoue A 2008 Mater. Sci. Eng. B 148 92
[9] He Y, Schwarz R B and Archuleta J I 1996 Appl. Phys. Lett. 69 1861
[10] Guo F Q, Poon S J and Shiflet G J 2003 Appl. Phys. Lett. 83 2575
[11] Li R, Pang S J, Ma C L and Zhang T 2007 Acta Mater. 55 3719
[12] Jiang Q K, Zhang G Q, Chen L Y, Wu J Z, Zhang H G and Jiang J Z 2006 J. Alloys Compd. 424 183
[13] Schroers J and Johnson W L 2004 Appl. Phys. Lett. 84 3666
[14] Ma H, Shi L L, Xu J, Li Y and Ma E 2005 Appl. Phys. Lett. 87 181915
[15] Shen J, Chen Q J, Sun J F, Fan H B and Wang G 2005 Appl. Phys. Lett. 86 151907
[16] Park E S and Kim D H 2004 J. Mater. Res. 19 685
[17] Busch R, Mauhr A, Bakke E and Johnson W L 1998 Mater. Sci. Forum 269–272 547
[18] Zhu S L, Wang X M and Inoue A 2008 Intermetallics 16 1031
[19] Xu D H, Duan G and Johnson W L 2004 Phys. Rev. Lett. 92 245504
[20] Men H, Pang S J and Zhang T 2006 J. Mater. Res. 21 958
[21] Pampillo C A and Chen H S 1974 Mater. Sci. Eng. 13 181
[22] Chen H S, Kimerling L C, Poate J M and Brown W L 1978 Appl. Phys. Lett. 32 461
[23] Steinberg J, Lord A E, Lacy L L and Johnson J 1981 Appl. Phys. Lett. 38 135
[24] Steinberg J, Tyagi S and Lord A E 1981 Appl. Phys. Lett. 38 878
[25] Yao K F, Ruan F 2005 Chin. Phys. Lett. 22 1481
[26] Yao K F, Ruan F, Yang Y Q and Chen N 2006 Appl. Phys. Lett. 88 122106
[27] Yao K F, Yang Y Q and Chen N 2007 Intermetallics 15 639
[28] Chen H S and Turnbull D 1969 Acta Metallurg. 17 1021