Effect of Quenching on the Grain Boundary Relaxation in PM2000 ODS Alloy

  • Grain boundary relaxation in a Fe-based ODS alloy is studied by internal friction measurements. It is found that a grain-boundary peak appears at a lower temperature in the quenched specimens than that in the annealed specimens. The activation energy of the peak is H=2.82±0.11eV for the former while H=2.53±0.08eV for the latter. In addition, a new relaxation peak is observed at the high temperature side of the grain boundary peak in the quenched specimens with an activation energy of 4.41±0.25eV. The height of the peak increases with increasing quenching temperature. The results suggest that both the shift of the grain-boundary peak and the appearance of the new peak are due to increasing vacancies by quenching that are favourable for the motion of the grain boundaries.
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