Stability Investigation of Colloidal FePt Nanoparticle Systems by Spectrophotometer Analysis
M. Farahmandjou1, S. A. Sebt1, S. S. Parhizgar1, P. Aberomand1, M. Akhavan2
1Physics Research Center, Science and Research Branch, Islamic Azad University, Tehran, Iran2Magnet Research Laboratories (MRL), Department of Physics, Sharif University of Technology, Tehran, Iran
Stability Investigation of Colloidal FePt Nanoparticle Systems by Spectrophotometer Analysis
M. Farahmandjou1, S. A. Sebt1, S. S. Parhizgar1, P. Aberomand1, M. Akhavan2
1Physics Research Center, Science and Research Branch, Islamic Azad University, Tehran, Iran2Magnet Research Laboratories (MRL), Department of Physics, Sharif University of Technology, Tehran, Iran
摘要FePt magnetic nanoparticle systems are an excellent candidate for ultrahigh-density magnetic recording. Monodisperse FePt nanoparticles are synthesized by superhydride reduction of FeCl212539;4H2O and Pt(acac)2 at 263°C under N2 atmosphere. Transmission electron microscopy (TEM) images show monosize FePt nanoparticles with diameter of 4nm and a standard deviation of about 10%. The average distance between monodispesre particles is nearly 3nm, and oleic acid and oleylamine surround the nanoparticles as surfactants. Stability investigation of nanoparticle colloidal solution is done via spectrophotometery analysis. The results for FePt nanoparticles dispersed in hexane indicate that adding surfactants with concentration of 3×10-3 part by volume for centrifugation stage increases the stability of FePt nanoparticles solution with concentration of 16mg/mL, about 67%.
Abstract:FePt magnetic nanoparticle systems are an excellent candidate for ultrahigh-density magnetic recording. Monodisperse FePt nanoparticles are synthesized by superhydride reduction of FeCl212539;4H2O and Pt(acac)2 at 263°C under N2 atmosphere. Transmission electron microscopy (TEM) images show monosize FePt nanoparticles with diameter of 4nm and a standard deviation of about 10%. The average distance between monodispesre particles is nearly 3nm, and oleic acid and oleylamine surround the nanoparticles as surfactants. Stability investigation of nanoparticle colloidal solution is done via spectrophotometery analysis. The results for FePt nanoparticles dispersed in hexane indicate that adding surfactants with concentration of 3×10-3 part by volume for centrifugation stage increases the stability of FePt nanoparticles solution with concentration of 16mg/mL, about 67%.
M. Farahmandjou;S. A. Sebt; S. S. Parhizgar;P. Aberomand;M. Akhavan. Stability Investigation of Colloidal FePt Nanoparticle Systems by Spectrophotometer Analysis[J]. 中国物理快报, 2009, 26(2): 27501-027501.
M. Farahmandjou, S. A. Sebt, S. S. Parhizgar, P. Aberomand, M. Akhavan. Stability Investigation of Colloidal FePt Nanoparticle Systems by Spectrophotometer Analysis. Chin. Phys. Lett., 2009, 26(2): 27501-027501.
[1] Nguyen L H et al 2005 J. Mater. Chem. 15 5136 [2] Liu P J et al 2006 IEEE Trans. Magn. 42 3036 [3] Sun S 2006 Adv. Mater. 18 393 [4] Elkins K et al 2005 J. Phys. D: Appl. Phys. 382306 [5] David Sellmyer and Ralf Skomski 2006 AdvancedMagnetic Nanostructures (Berlin: Springer) p 239 [6] Shan Wang and Alexander Taratorin 1999 MagneticInformation Storage Technology (New York: Academic) p 177 [7] Christodoulides A J et al 2003 Phys. Rev. B 68054428 [8] Sun S et al 2003 J. Phys. Chem. B 107 5419 [9] V\'{azquez M et al 2004 Physica B 354 71 [10] Acet M et al 2005 J. Cryst. Growth 285 365 [11] Scherer C, Neto F A 2005 Braz. J. Phys. 35 718 [12] Shukla N et al 2007 Colloids and Surfaces A 301 113 [13] Shukla N et al 2004 J. Magn. Magn. Mater. 272e1349 [14] Klokkenburg M et al 2007 Vibration. Spectrosc. 43 243 [15] Zoriasatain S et al 2006 J. Magn. Magn. Mater 300 526